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9 months ago
733 B
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Mixture of benzoic acid + 4-(benzyloxy)phenol + biphenyl
            │
   Dissolve in ether (organic solvent)
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 Add NaHCO₃ (weak base) → extracts benzoic acid → aqueous layer (Na⁺ benzoate)
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 Acidify with HCl → benzoic acid precipitates → isolate by vacuum filtration
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Remaining organic layer → Add NaOH (strong base)
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 Extracts phenol → aqueous layer (phenoxide ion)
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 Acidify with HCl → 4-(benzyloxy)phenol precipitates → isolate by vacuum filtration
            │
Remaining ether layer → contains biphenyl
            │
 Dry with MgSO₄ → gravity filter → rotary evaporate ether
            ↓
           Crude biphenyl

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